STRUCTURE OF 1,2,3-TRIS(DIMETHYLAMINO)CYCLOPROPENYLIUM AQUATETRACHLOROOXONIOBATE(V)

被引：16

作者：

SCHAFER, HN ^{[1
]}

BURZLAFF, H ^{[1
]}

GRIMMEISS, AMH ^{[1
]}

WEISS, R ^{[1
]}

机构：

[1] UNIV ERLANGEN NURNBERG,INST ORGAN CHEM,LEHRSTUHL 1,W-8520 ERLANGEN,GERMANY

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1991年 / 47卷

关键词：

D O I：

10.1107/S0108270191001245

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

[C9H18N3][NbCl4O(H2O)], M(r) = 436.997, triclinic, P1, a = 12.2716 (9), b = 8.9682 (5), c = 8.7625 (5) angstrom, alpha = 70.203 (9), beta = 88.242 (5), gamma = 71.299 (5)-degrees, V = 856.137 angstrom 3, Z = 2, D(x) = 1.695 g cm-3, Mo K-alpha, lambda = 0.70926 angstrom, mu = 13.042 cm-1, F(000) = 440, room temperature, final [GRAPHICS] R = 0.0344 for F and 2141 reflections. The crystal structure consists of chains of [NbOCl4(OH2)]-square bipyramids along the [110] direction connected by trigonal planar [C3{N(CH3)2}3]+ ions.

引用

页码：1808 / 1811

页数：4

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