DETERMINATION OF METHYL CARBAMATE RESIDUES USING ONLINE COUPLING OF HPLC WITH A POST COLUMN FLUOROMETRIC LABELING TECHNIQUE

被引：20

作者：

BLASS, W

机构：

[1] Institut für Rückstandsanalytik, Bayer AG, Leverkusen

来源：

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1991年 / 339卷 / 06期

关键词：

D O I：

10.1007/BF00322345

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

An HPLC method for post-column derivatisation and on-line coupled fluorescence detection of N-methyl-carbamates is presented. Some improvements of the original procedure described in the literature [1-7] are reported. 26 different sample materials and the same number of compounds were analysed by this method. High selectivity, high sensitivity, the determination of unchanged compounds and metabolites in one run, and a considerable saving of analysis time are the main features of the method.

引用

页码：340 / 343

页数：4

共 7 条

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[4] KRAUSE RT, 1980, J ASSOC OFF ANA CHEM, V63, P1114
[5] KRAUSE RT, 1985, J ASSOC OFF ANA CHEM, V68, P726
[6] RESOLUTION, SENSITIVITY AND SELECTIVITY OF A HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC POST-COLUMN FLUOROMETRIC LABELING TECHNIQUE FOR DETERMINATION OF CARBAMATE INSECTICIDES
KRAUSE, RT
[J]. JOURNAL OF CHROMATOGRAPHY, 1979, 185 (DEC): : 615 - 624
[7] DYNAMIC FLUOROGENIC LABELING OF PESTICIDES FOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY - DETECTION OF N-METHYLCARBAMATES WITH ORTHO-PHTHALALDEHYDE
MOYE, HA
SCHERER, SJ
STJOHN, PA
[J]. ANALYTICAL LETTERS, 1977, 10 (13) : 1049 - 1073

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