CRYSTAL-STRUCTURE OF GEF4

被引：18

作者：

KOHLER, J ^{[1
]}

SIMON, A ^{[1
]}

HOPPE, R ^{[1
]}

机构：

[1] UNIV GIESSEN, D-6300 GIESSEN, FED REP GER

来源：

JOURNAL OF THE LESS-COMMON METALS | 1988年 / 137卷 / 1-2期

关键词：

CRYSTALS; -; Structure;

D O I：

10.1016/0022-5088(88)90098-7

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

GeF//4 has been prepared by heating BaGeF//6 at 600 degree C under a pressure of 10** minus **3 Torr and has been solidified by cooling with liquid nitrogen in a quartz ampoule. A small amount was sealed in a quartz capillary and it was shown that a single crystal could be grown from the gas phase on a four-circle diffractometer at minus 30 degree C. The crystal structure and the calculated Madelung part of lattice energy (MAPLE) are discussed.

引用

页码：333 / 341

页数：9

共 37 条

[1] CRYSTAL-STRUCTURES OF [XE2F3+][ASF6-] AND [XEF5+][ASF6-] [J].

BARTLETT, N ;

DEBOER, BG ;

HOLLANDE.FJ ;

SLADKY, FO ;

TEMPLETO.DH ;

ZALKIN, A .

INORGANIC CHEMISTRY, 1974, 13 (04) :780-785

[2] RUTILE-TYPE COMPOUNDS .4. SIO2, GEO2 AND A COMPARISON WITH OTHER RUTILE-TYPE STRUCTURES [J].

BAUR, WH ;

KHAN, AA .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL CRYSTALLOGRAPHY AND CRYSTAL CHEMISTRY, 1971, B 27 (NOV15) :2133-&

[3] CRYSTAL-STRUCTURE OF ALPHA-CF4 [J].

BOLSHUTKIN, DN ;

GASAN, VM ;

PROKHVATILOV, AI ;

ERENBURG, AI .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 1972, 28 (DEC15) :3542-3547

[4]

BRAUERN GM, 1966, ACTA CRYSTALLOGR, V20, P220

[5] FRAGMENTATION AND AGGREGATION ON LEAD-OXIDES - ON THE OLIGOOXOPLUMBATE(IV) K2LI6[PB2O8] [J].

BRAZEL, B ;

HOPPE, R .

ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1983, 497 (02) :176-184

[6]

BROWN JD, 1985, ACTA CRYSTALLOGR B, V41, P241

[7] CRYSTAL STRUCTURES OF POTASSIUM, AMMONIUM, RUBIDIUM, AND CESIUM TETRAFLUOBORATES [J].

CLARK, MJR ;

LYNTON, H .

CANADIAN JOURNAL OF CHEMISTRY, 1969, 47 (14) :2579-&

[8] ABOUT SNF2 STANNOUS FLUORIDE .1. CRYSTALLOCHEMISTRY OF ALPHA-SNF2 [J].

DENES, G ;

PANNETIER, J ;

LUCAS, J ;

LEMAROUILLE, JY .

JOURNAL OF SOLID STATE CHEMISTRY, 1979, 30 (03) :335-343

[9]

EDWARDS WJ, 1971, CHEM COMMUN, P1376

[10] POTASSIUM ARSENIC HEXAFLUORINE - REDETERMINATION [J].

GAFNER, G ;

KRUGER, GJ .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1974, B 30 (JAN15) :250-251

← 1 2 3 4 →