ISOTHERMAL IN-SITU REDUCTION KINETIC-ANALYSIS OF NICL2-CONTAINING GEL

被引:10
作者
DAS, GC [1 ]
BASUMALLICK, A [1 ]
SEN, KB [1 ]
MUKHERJEE, S [1 ]
机构
[1] BENGAL ENGN COLL,DEPT MET ENGN,HOWRAH 711103,W BENGAL,INDIA
关键词
IN-SITU REDUCTION; ISOTHERMAL KINETICS; NANOCOMPOSITES; SOL-GEL;
D O I
10.1007/BF02746042
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Isothermal in situ reduction kinetic study of NiCl2-containing gel was carried out. The detailed statistical as well as reduced time analysis show that contracting geometry and nucleation and growth type of mixed mechanisms are operative. The activation energy for reduction is in the range 158-193 kJ/mol. Thermal analysis on NiCl2-containing gel was carried out in the temperature range 800-degrees-C to 900-degrees-C.
引用
收藏
页码:317 / 324
页数:8
相关论文
共 9 条
[1]   SOL-GEL TRANSITION IN SIMPLE SILICATES [J].
BRINKER, CJ ;
KEEFER, KD ;
SCHAEFER, DW ;
ASHLEY, CS .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 1982, 48 (01) :47-64
[2]   NANOCOMPOSITES [J].
CHAKRAVORTY, D .
BULLETIN OF MATERIALS SCIENCE, 1992, 15 (05) :411-420
[3]   ELECTRICAL-CONDUCTION IN SOL-GEL DERIVED GLASS METAL NANOCOMPOSITES [J].
CHATTERJEE, A ;
CHAKRAVORTY, D .
JOURNAL OF PHYSICS D-APPLIED PHYSICS, 1990, 23 (08) :1097-1102
[4]   GLASS METAL NANOCOMPOSITE SYNTHESIS BY METAL ORGANIC ROUTE [J].
CHATTERJEE, A ;
CHAKRAVORTY, D .
JOURNAL OF PHYSICS D-APPLIED PHYSICS, 1989, 22 (09) :1386-1392
[5]   CLUSTER EFFECTS ON OPTICAL-PROPERTIES OF GLASS METAL NANOCOMPOSITES [J].
DAS, GC ;
CHAKRAVORTY, D .
BULLETIN OF MATERIALS SCIENCE, 1989, 12 (05) :449-456
[6]   PREPARATION OF GLASS NICKEL MICROCOMPOSITES BY INSITU REDUCTION VIA SOL-GEL ROUTE [J].
DAS, GC ;
BASUMALLICK, A ;
MUKHERJEE, S .
BULLETIN OF MATERIALS SCIENCE, 1990, 13 (04) :255-258
[7]  
DUTTA S, 1984, J PHYS D, V17, P163
[8]  
KEATTCH CJ, 1975, INTRO THERMOGRAVIMET, P57
[9]  
PERRY RH, 1983, CHEM ENG HDB, P3