SYNTHESIS OF 2-SUBSTITUTED-4H-3,1-BENZOXAZIN-4-ONES

被引：94

作者：

BAIN, DI

SMALLEY, RK

机构：

[1] Department of Pure and Applied Chemistry, University of Salford, Salford

来源：

JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC | 1968年 / 13期

关键词：

D O I：

10.1039/j39680001593

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Anthranilic acid (1 mol.) reacted in pyridine solution with benzoyl chloride (2 mol.) to give 2-phenyl-4H-3,1-benzoxazin-4-one in high yield. With 1 mol. of benzoyl chloride, however, a mixture of benzoxazinone and N-benzoylanthranilic acid was obtained. The mechanism of the reaction has been investigated and various 2-substituted-4H-3,1 -benzoxazin-4-ones have been prepared and their u.v. spectra recorded.

引用

页码：1593 / &

共 12 条

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