SENSITIVE PULSED EPR SPECTROMETER WITH AN 8-18 GHZ FREQUENCY-RANGE

被引:56
作者
STURGEON, BE
BRITT, RD
机构
关键词
D O I
10.1063/1.1143136
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
The design and construction details of a kW power level pulsed EPR spectrometer with an 8-18 GHz frequency range are presented. The spectrometer is designed for high sensitivity over this wide frequency range. A synthesized sweeper is used as the microwave source. Details of the pulse electronics, pulse timings, cryogenics, and the Macintosh computer interface are described. Representative three pulse electron spin echo envelope modulation patterns of a Cu (II) tetraimidazole complex at X- and P-band frequencies are presented.
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页码:2187 / 2192
页数:6
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