TEMPERATURE CONTROLLED MICROWAVE-OVEN DIGESTION SYSTEM

被引:13
作者
MINCEY, DW
WILLIAMS, RC
GIGLIO, JJ
GRAVES, GA
PACELLA, AJ
机构
[1] Department of Chemistry, Youngstown State University, Youngstown
关键词
MICROWAVE OVEN; DIGESTION SYSTEM;
D O I
10.1016/0003-2670(92)85301-L
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Microwave oven digestion of samples for elemental analysis is becoming a widely used laboratory technique. The employment of sealed pressurized vessels has reduced the time required to place samples into solution. However, the incomplete dissolution of hard to digest materials remains a problem. In our laboratories, the digestion of biological specimens such as leaves and insect matter, result in a white precipitate after dilution. A similar digestion on a hotplate produces a clear solution.
引用
收藏
页码:97 / 100
页数:4
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KINGSTON, HM ;
JASSIE, LB .
ANALYTICAL CHEMISTRY, 1986, 58 (12) :2534-2541
[3]  
NICHOLSON JRP, 1989, CLIN CHEM, V35, P3