SEPARATION OF DIPOLAR AND QUADRUPOLAR SPLITTINGS IN SINGLE-CRYSTAL N-14 NMR

被引:34
作者
BODENHAUSEN, G
STARK, RE
RUBEN, DJ
GRIFFIN, RG
机构
[1] Francis Bitter National Magnet Laboratory, Massachusetts Institute of Technology, Cambridge
基金
美国国家卫生研究院; 美国国家科学基金会;
关键词
D O I
10.1016/0009-2614(79)85194-5
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A new two-dimensional Fourier transform technique is proposed to unravel overlapping resonances in single crystal 14N spectra due to proton-nitrogen dipolar couplings. One frequency domain is reserved for the proton decoupled quadrupolar spectrum, while the orthogonal frequency dimension shows the dipolar splittings alone, the quadrupolar interaction being eliminated by refocusing. © 1979.
引用
收藏
页码:424 / 427
页数:4
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