SIMULTANEOUS DETERMINATION OF RESIDUES OF FLORFENICOL AND THE METABOLITE FLORFENICOL AMINE IN FISH-TISSUES BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引:41
作者
HORMAZABAL, V [1 ]
STEFFENAK, I [1 ]
YNDESTAD, M [1 ]
机构
[1] NORWEGIAN COLL VET MED,DEPT FOOD HYG,POB 8146 DEP,N-0033 OSLO 1,NORWAY
来源
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS | 1993年 / 616卷 / 01期
关键词
D O I
10.1016/0378-4347(93)80484-L
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A simple and rapid high-performance liquid chromatographic method for the simultaneous extraction and determination of residues of florfenicol and its metabolite florfenicol amine in fish tissue, muscle and liver has been developed. The calibration curves were linear, the recovery of florfenicol was 99-107%, and the recovery of florfenicol amine was 94-100%. The detection limits for florfenicol and florfenicol amine were 20 ng/g in muscle and 50 ng/g in liver.
引用
收藏
页码:161 / 165
页数:5
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