N-METHYLIMIDAZOLE-CATALYZED ACETYLATION OF HYDROXY COMPOUNDS PRIOR TO GAS-CHROMATOGRAPHIC SEPARATION AND DETERMINATION

被引：45

作者：

WACHOWIAK, R ^{[1
]}

CONNORS, KA ^{[1
]}

机构：

[1] UNIV WISCONSIN,SCH PHARM,MADISON,WI 53706

来源：

ANALYTICAL CHEMISTRY | 1979年 / 51卷 / 01期

关键词：

D O I：

10.1021/ac50037a014

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Alcohols, phenols, glycols, and sugars were quantitatively acetylated in about 5 min at room temperature with acetic anhydride in the presence of N-methylimidazole. Gas chromatographic conditions are described for the separation and determination of the acetylated products. © 1979, American Chemical Society. All rights reserved.

引用

页码：27 / 30

页数：4

共 16 条

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