SUPPRESSION OF SIDE-BAND IN MAGIC-ANGLE-SPINNING NUCLEAR-MAGNETIC-RESONANCE - GENERAL-PRINCIPLES AND ANALYTICAL SOLUTIONS

被引：48

作者：

ANTZUTKIN, ON

SONG, ZY

FENG, XL

LEVITT, MH

机构：

[1] Division of Physical Chemistry, Arrhenius Laboratory, University of Stockholm

来源：

JOURNAL OF CHEMICAL PHYSICS | 1994年 / 100卷 / 01期

关键词：

D O I：

10.1063/1.466983

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 [物理化学]; 081704 [应用化学];

摘要：

Several theoretical and experimental aspects of sideband suppression in the nuclear magnetic resonance (NMR) spectra of rotating solids are considered. The principles of sideband suppression are explored using general symmetry arguments and previous treatments are examined critically. Analytical solutions are given for sideband suppression pulse sequences employing four, five, six, and nine pi pulses. The analytical solutions for four pi pulses are complete. Experimental demonstrations are given.

引用

收藏

页码：130 / 140

页数：11

相关论文

共 21 条

[1]

SELECTION OF COHERENCE-TRANSFER PATHWAYS IN NMR PULSE EXPERIMENTS [J].

BODENHAUSEN, G ;

KOGLER, H ;

ERNST, RR .

JOURNAL OF MAGNETIC RESONANCE, 1984, 58 (03) :370-388

[2]

SELECTIVE PULSE EXPERIMENTS IN HIGH-RESOLUTION SOLID-STATE NMR [J].

CARAVATTI, P ;

BODENHAUSEN, G ;

ERNST, RR .

JOURNAL OF MAGNETIC RESONANCE, 1983, 55 (01) :88-103

[3]

DIXON WT, 1985, J MAGN RESON, V64, P332, DOI 10.1016/0022-2364(85)90359-2

[4]

TOTAL SUPPRESSION OF SIDEBANDS IN CPMAS C-13 NMR [J].

DIXON, WT ;

SCHAEFER, J ;

SEFCIK, MD ;

STEJSKAL, EO ;

MCKAY, RA .

JOURNAL OF MAGNETIC RESONANCE, 1982, 49 (02) :341-345

[5]

SPINNING-SIDEBAND-FREE AND SPINNING-SIDEBAND-ONLY NMR-SPECTRA IN SPINNING SAMPLES [J].

DIXON, WT .

JOURNAL OF CHEMICAL PHYSICS, 1982, 77 (04) :1800-1809

[6]

PURE ABSORPTION-MODE CHEMICAL-EXCHANGE NUCLEAR-MAGNETIC-RESONANCE SPECTROSCOPY WITH SUPPRESSION OF SPINNING SIDE-BAND IN A SLOWLY ROTATING SOLID [J].

GEEN, H ;

BODENHAUSEN, G .

JOURNAL OF CHEMICAL PHYSICS, 1992, 97 (05) :2928-2937

[7]

COMPLETE SIDE-BAND SUPPRESSION IN MAGIC ANGLE SPINNING SOLID-STATE NUCLEAR-MAGNETIC-RESONANCE FOR ARBITRARY CHEMICAL-SHIFT ANISOTROPIES [J].

GEEN, H ;

BODENHAUSEN, G .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1993, 115 (04) :1579-1580

[8]

HAGEMEYER A, 1989, ADV MAGN RESON, V13, P85

[9]

SUPPRESSION OF SPINNING SIDEBANDS IN MAGIC-ANGLE-SPINNING NMR-SPECTROSCOPY USING 180-DEGREE PULSES - AN APPLICATION TO BIOLOGICAL-SYSTEMS [J].

HEMMINGA, MA ;

DEJAGER, PA .

JOURNAL OF MAGNETIC RESONANCE, 1983, 51 (02) :339-344

[10]

HONG J, IN PRESS J MAGN RESO