REMOVAL OF T-BUTYLDIMETHYLSILYL PROTECTION IN RNA-SYNTHESIS - TRIETHYLAMINE TRIHYDROFLUORIDE (TEA, 3HF) IS A MORE RELIABLE ALTERNATIVE TO TETRABUTYLAMMONIUM FLUORIDE (TBAF)

被引：105

作者：

WESTMAN, E ^{[1
]}

STROMBERG, R ^{[1
]}

机构：

[1] UNIV STOCKHOLM,ARRHENIUS LAB,DEPT ORGAN CHEM,S-10691 STOCKHOLM,SWEDEN

来源：

NUCLEIC ACIDS RESEARCH | 1994年 / 22卷 / 12期

关键词：

D O I：

10.1093/nar/22.12.2430

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

引用

页码：2430 / 2431

页数：2

共 11 条

[1] SYNTHESIS OF DIRIBONUCLEOSIDE PHOSPHOROTHIOATES VIA STEREOSPECIFIC SULFURIZATION OF H-PHOSPHONATE DIESTERS [J].

ALMER, H ;

STAWINSKI, J ;

STROMBERG, R ;

THELIN, M .

JOURNAL OF ORGANIC CHEMISTRY, 1992, 57 (23) :6163-6169

[2] NUCLEOSIDE H-PHOSPHONATES .4. AUTOMATED SOLID-PHASE SYNTHESIS OF OLIGORIBONUCLEOTIDES BY THE HYDROGENPHOSPHONATE APPROACH [J].

GAREGG, PJ ;

LINDH, I ;

REGBERG, T ;

STAWINSKI, J ;

STROMBERG, R ;

HENRICHSON, C .

TETRAHEDRON LETTERS, 1986, 27 (34) :4055-4058

[3] CHEMICAL SYNTHESIS OF A BIOLOGICALLY-ACTIVE NATURAL TRANSFER-RNA WITH ITS MINOR BASES [J].

GASPARUTTO, D ;

LIVACHE, T ;

BAZIN, H ;

DUPLAA, AM ;

GUY, A ;

KHORLIN, A ;

MOLKO, D ;

ROGET, A ;

TEOULE, R .

NUCLEIC ACIDS RESEARCH, 1992, 20 (19) :5159-5166

[4] EFFECT OF EXCESS WATER ON THE DESILYLATION OF OLIGORIBONUCLEOTIDES USING TETRABUTYLAMMONIUM FLUORIDE [J].

HOGREFE, RI ;

MCCAFFREY, AP ;

BOROZDINA, LU ;

MCCAMPBELL, ES ;

VAGHEFI, MM .

NUCLEIC ACIDS RESEARCH, 1993, 21 (20) :4739-4741

[5] EVALUATION OF 2'-HYDROXYL PROTECTION IN RNA-SYNTHESIS USING THE H-PHOSPHONATE APPROACH [J].

ROZNERS, E ;

WESTMAN, E ;

STROMBERG, R .

NUCLEIC ACIDS RESEARCH, 1994, 22 (01) :94-99

[6] STUDIES ON THE TERT-BUTYLDIMETHYLSILYL GROUP AS 2'-O-PROTECTION IN OLIGORIBONUCLEOTIDE SYNTHESIS VIA THE H-PHOSPHONATE APPROACH [J].

STAWINSKI, J ;

STROMBERG, R ;

THELIN, M ;

WESTMAN, E .

NUCLEIC ACIDS RESEARCH, 1988, 16 (19) :9285-9298

[7] AUTOMATED CHEMICAL SYNTHESIS OF LONG OLIGORIBONUCLEOTIDES USING 2'-O-SILYLATED RIBONUCLEOSIDE 3'-O-PHOSPHORAMIDITES ON A CONTROLLED-PORE GLASS SUPPORT - SYNTHESIS OF A 43-NUCLEOTIDE SEQUENCE SIMILAR TO THE 3'-HALF MOLECULE OF AN ESCHERICHIA-COLI FORMYLMETHIONINE TRANSFER-RNA [J].

USMAN, N ;

OGILVIE, KK ;

JIANG, MY ;

CEDERGREN, RJ .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1987, 109 (25) :7845-7854

[8] PREPARATION OF RIBONUCLEOSIDE 3'-O-PHOSPHORAMIDITES AND THEIR APPLICATION TO THE AUTOMATED SOLID-PHASE SYNTHESIS OF OLIGONUCLEOTIDES [J].

USMAN, N ;

PON, RT ;

OGILVIE, KK .

TETRAHEDRON LETTERS, 1985, 26 (38) :4567-4570

[9]

WESTMAN E, CHEM COMPONENTS NUCL

[10]

WESTMAN E, 1993, SEP CHEM COMP NUCL A

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