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MERCURATION OF A RUTHENOCENE - SYNTHESIS, CHARACTERIZATION, AND HALOGENATION OF [(C5(HGO2CCH3)5)(C5(CH3)5)RU]

被引：32
作者：
WINTER, CH
HAN, YH
HEEG, MJ
机构：
[1] Department of Chemistry, Wayne State University, Detroit
来源：
ORGANOMETALLICS | 1992年 / 11卷 / 10期
关键词：
D O I：
10.1021/om00046a006
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Treatment of pentamethylruthenocene with 5 equiv of mercuric acetate affords pentakis(acetoxymecurio)pentamethylruthenocene (88%), which can be halogenated with potassium triiodide or potassium tribromide to afford pentaiodopentamethylruthenocene (60%) and pentabromopentamethylruthenocene (35%). The crystal structure of the pentaiodopentamethylruthenocene derivative is described.
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页码：3169 / 3171
页数：3
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