SATURABLE INDUCTOR BASED CONTROLLED WAVEFORM EXCITATION SOURCE FOR EXPLODING THIN-FILM ATOMIC SPECTROSCOPY

被引:22
作者
SUH, SY [1 ]
COLLINS, RJ [1 ]
SACKS, RD [1 ]
机构
[1] UNIV MICHIGAN,DEPT CHEM,ANN ARBOR,MI 48109
关键词
D O I
10.1366/0003702814731969
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
An adjustable waveform excitation source for exploding thin film atomic spectroscopy is described. Waveform control is achieved through a saturable inductor having control windings and placed in series with the underdamped discharge tank circuit. This results in a high-current pulse for efficient sample atomization followed by a low-current measurement interval. When this is combined with gated integration, approximately 15-fold increases in analysis line/background intensity ratios are observed for V and Mn. With additional inductance added to the circuit, the current and duration of both the atomization pulse and measurement interval can be adjusted independently.
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页码:42 / 52
页数:11
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