SIMPLE, RAPID AND SIMULTANEOUS MEASUREMENT OF 8 DIFFERENT TYPES OF CARBAMATE PESTICIDES IN SERUM USING LIQUID-CHROMATOGRAPHY ATMOSPHERIC-PRESSURE CHEMICAL-IONIZATION MASS-SPECTROMETRY

被引：29

作者：

KAWASAKI, S ^{[1
]}

NAGUMO, F ^{[1
]}

UEDA, H ^{[1
]}

TAJIMA, Y ^{[1
]}

SANO, M ^{[1
]}

TADANO, J ^{[1
]}

机构：

[1] SAGA MED SCH HOSP,DEPT LAB MED,5-1-1 NABESHIMA,SAGA 849,JAPAN

来源：

JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS | 1993年 / 620卷 / 01期

关键词：

D O I：

10.1016/0378-4347(93)80052-6

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

We have developed a method for simultaneous analysis of methylcarbamate pesticides in serum with an acute pesticide intoxication. This is performed by liquid chromatography-atmospheric pressure chemical ionization mass spectrometry. Rapid detection of eight types of methylcarbamate pesticide can be achieved with this method, it only requires an extremely simple pre-treatment of the sample. The specificity of this method is equal to that of gas chromatography-mass spectrometry, and it satisfies the clinical requirements for detection sensitivity and specificity. Although some problems with this analytical method remain to be solved, we consider it to be superior to any other analytical method previously reported.

引用

页码：61 / 71

页数：11

共 20 条

[1] PERSISTENCE AND METABOLISM OF ALDICARB IN FRESH POTATOES [J].

CAIRNS, T ;

SIEGMUND, EG ;

SAVAGE, TS .

BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY, 1984, 32 (03) :274-281

[2]

CHEN JYT, 1966, J ASSOC OFF ANA CHEM, V49, P412

[3]

COLVIN BM, 1974, J ASSOC OFF ANA CHEM, V57, P648

[4]

HORGAN DG, 1974, ANAL METHODS PESTICI, V7, pCH2

[5]

ISHII Y, 1973, B AGR CHEM INSP STA, V13, P32

[6] CHLORIDE ATTACHMENT NEGATIVE-ION MASS-SPECTRA OF SUGARS BY COMBINED LIQUID-CHROMATOGRAPHY AND ATMOSPHERIC-PRESSURE CHEMICAL IONIZATION MASS-SPECTROMETRY [J].

KATO, Y ;

NUMAJIRI, Y .

JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1991, 562 (1-2) :81-97

[7] SCREENING OF ORGANOPHOSPHORUS PESTICIDES USING LIQUID-CHROMATOGRAPHY ATMOSPHERIC-PRESSURE CHEMICAL IONIZATION MASS-SPECTROMETRY [J].

KAWASAKI, S ;

UEDA, H ;

ITOH, H ;

TADANO, J .

JOURNAL OF CHROMATOGRAPHY, 1992, 595 (1-2) :193-202

[8] METHOD FOR HIGH-SPEED LIQUID CHROMATOGRAPHIC ANALYSIS OF BENOMYL AND/OR METABOLITE RESIDUES IN COW MILK, URINE, FECES, AND TISSUES [J].

KIRKLAND, JJ .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1973, 21 (02) :171-177

[9] DETERMINATION OF BENOMYL RESIDUES IN SOILS AND PLANT-TISSUES BY HIGH-SPEED CATION-EXCHANGE LIQUID CHROMATOGRAPHY [J].

KIRKLAND, JJ ;

HOLT, RF ;

PEASE, HL .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1973, 21 (03) :368-371

[10] GAS-CHROMATOGRAPHIC ANALYSIS OF CHLOROQUINE AFTER A UNIQUE REACTION WITH CHLOROFORMATES [J].

KUYE, JO ;

WILSON, MJ ;

WALLE, T .

JOURNAL OF CHROMATOGRAPHY, 1983, 272 (02) :307-313

← 1 2 →