PYROLYSIS-GAS CHROMATOGRAPHIC ANALYSES OF ORGANIC-MATTER IN SOILS USING NITROGEN-SELECTIVE DETECTION

被引:14
作者
GRANADA, E
BLASCO, J
COMELLAS, L
GASSIOT, M
机构
[1] Secc. Cromatografia, Dep. Quim. Analitica CETS Institut Quimic de Sarria (centre associat al CSIC)
关键词
GAS CHROMATOGRAPHIC SEPARATION; ORGANIC MATTER; NITROGEN-SELECTIVE DETECTION; PYROLYSIS; SOILS;
D O I
10.1016/0165-2370(91)80043-8
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Pyrolysis in combination with gas-chromatographic separation and nitrogen selective detection is proposed for the analysis of nitrogen compounds in soils. The technique is considered as a complementary tool besides other techniques for soil organic matter studies. The pyrolysis probe has been placed directly into the injection port of a HP5890A chromatograph coupled with a nitrogen selective detector. The linearity and reproducibility obtained with this configuration were comparable to those obtained with a FID detection. Also a better sensitivity was observed.
引用
收藏
页码:193 / 202
页数:10
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