IDENTIFICATION OF ACETYL DERIVATIVE ISOMERS OF 1,5-ANHYDRO-D-XYLITOL BY GAS-CHROMATOGRAPHY AND MASS-SPECTROMETRY

被引：5

作者：

SZAFRANEK, J

WISNIEWSKI, A

GAJDUS, J

KUSMIERZ, J

机构：

[1] Mass Spectrometry Laboratory, University of Gdańsk, 80-952 Gdańsk

来源：

JOURNAL OF CHROMATOGRAPHY | 1979年 / 168卷 / 02期

关键词：

D O I：

10.1016/0021-9673(79)80015-1

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

High-resolution gas chromatography and mass spectrometry have been employed to separate selectively acetylated 1,5-anhydro-d-xylitol derivatives and to study their chemical structures. Complete separation of reaction mixtures was achieved on a capillary column coated with an SE-30 liquid phase. The combination of gas chromatography-mass spectrometry with oxidation reactions allowed the assignment of the chemical structures of all the derivatives, obtained. © 1979.

引用

页码：445 / 453

页数：9

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