ONLINE PRECONCENTRATION AND ION CHROMATOGRAPHY OF TRIAZINE COMPOUNDS

被引：22

作者：

SACCHERO, G ^{[1
]}

SARZANINI, C ^{[1
]}

MENTASTI, E ^{[1
]}

机构：

[1] UNIV TURIN,DEPT ANALYT CHEM,I-1025 TURIN,ITALY

来源：

JOURNAL OF CHROMATOGRAPHY A | 1994年 / 671卷 / 1-2期

关键词：

D O I：

10.1016/0021-9673(94)80233-5

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

An ion chromatographic method was developed for the determination of triazine herbicides in environmental samples. Considering the polar nature of triazines, a cation-exchange column with a multi-mode pellicular packing was used. Optimization of the eluent (organic modifier concentration and ionic strength) is described with reference to the separation, on-line dean-up and preconcentration procedure. Several enrichment materials were evaluated and detection limits below 100 ng/l were achieved with a reversed-phase silica. The determination of triazines in tap water and river water samples was performed with UV detection (220 or 263 nm).

引用

收藏

页码：151 / 157

页数：7

相关论文

共 15 条

[1] DETERMINATION OF TRIAZINE HERBICIDES IN SURFACE AND DRINKING WATERS BY OFF-LINE COMBINATION OF LIQUID-CHROMATOGRAPHY AND GAS-CHROMATOGRAPHY MASS-SPECTROMETRY [J].

BAGHERI, H ;

VREULS, JJ ;

GHIJSEN, RT ;

BRINKMAN, UAT .

CHROMATOGRAPHIA, 1992, 34 (1-2) :5-13

[2] A REVIEW OF LIQUID-CHROMATOGRAPHY IN ENVIRONMENTAL PESTICIDE ANALYSIS [J].

BARCELO, D .

CHROMATOGRAPHIA, 1988, 25 (10) :928-936

[3] INFLUENCE OF REVERSED-PHASE AND NORMAL-PHASE LIQUID-CHROMATOGRAPHIC ELUENTS IN THE FRAGMENTATION OF SELECTED CHLORINATED HERBICIDES IN THERMOSPRAY LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY [J].

BARCELO, D .

ORGANIC MASS SPECTROMETRY, 1989, 24 (10) :898-902

[4] EXTRACTION AND ISOLATION OF TRIAZINE HERBICIDES FROM WATER AND VEGETABLES BY A DOUBLE TRAP TANDEM SYSTEM [J].

BATTISTA, M ;

DICORCIA, A ;

MARCHETTI, M .

ANALYTICAL CHEMISTRY, 1989, 61 (09) :935-939

[5] DETERMINATION OF POLAR POLLUTANTS IN WATER USING AN ONLINE LIQUID-CHROMATOGRAPHIC PRECONCENTRATION SYSTEM [J].

BROUWER, ER ;

LISKA, I ;

GEERDINK, RB ;

FRINTROP, PCM ;

MULDER, WH ;

LINGEMAN, H ;

BRINKMAN, UAT .

CHROMATOGRAPHIA, 1991, 32 (9-10) :445-452

[6] DETERMINATION OF CHLOROTRIAZINES IN AQUEOUS ENVIRONMENTAL-SAMPLES AT THE NG/1 LEVEL USING PRECONCENTRATION WITH A CATION EXCHANGER AND ONLINE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].

COQUART, V ;

HENNION, MC .

JOURNAL OF CHROMATOGRAPHY, 1991, 585 (01) :67-73

[7] DETERMINATION OF CHLOROTRIAZINES AND THEIR PHOTOLYSIS PRODUCTS BY LIQUID-CHROMATOGRAPHY WITH PHOTODIODE-ARRAY AND THERMOSPRAY MASS-SPECTROMETRIC DETECTION [J].

DURAND, G ;

BARCELO, D .

JOURNAL OF CHROMATOGRAPHY, 1990, 502 (02) :275-286

[8] HIGH-PERFORMANCE-LIQUID CHROMATOGRAPHIC-SEPARATION OF 1,3,5-TRIAZINE HERBICIDES [J].

GUNTHER, WJ ;

KETTRUP, A .

CHROMATOGRAPHIA, 1989, 28 (3-4) :209-211

[9] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF ATRAZINE, DEISOPROPYLATRAZINE AND DEETHYLATRAZINE IN SOILS FROM CORN FIELDS [J].

KARLAGANIS, G ;

VONARX, R ;

AMMON, HU ;

CAMENZIND, R .

JOURNAL OF CHROMATOGRAPHY, 1991, 549 (1-2) :229-236

[10]

LISKA I, 1989, HRC-J HIGH RES CHROM, V12, P577