PACKED MICROCAPILLARY COLUMNS WITH DIFFERENT SELECTIVITIES FOR LIQUID-CHROMATOGRAPHY

被引:72
作者
HIRATA, Y
NOVOTNY, M
TSUDA, T
ISHII, D
机构
[1] INDIANA UNIV,DEPT CHEM,BLOOMINGTON,IN 47405
[2] NAGOYA UNIV,FAC ENGN,DEPT APPL CHEM,CHIKUSA KU,NAGOYA,AICHI 464,JAPAN
关键词
D O I
10.1021/ac50047a046
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Packed microcapillary columns for high-performance LC are prepared by drawing alumina or silica particles inside the thick-walled glass tubing, and a subsequent in situ bonding of various silanes to their surfaces. The columns with different selectivities were prepared, including a polar phase, a re-versed-phase column, and an ion-exchanger packing. Chromatographic results are presented with standard solutes. Microcolumns with different selectivities and very high efficiencies are now available. © 1979, American Chemical Society. All rights reserved.
引用
收藏
页码:1807 / 1809
页数:3
相关论文
共 12 条
[1]   PREPARATION AND CHROMATOGRAPHIC EVALUATION OF CHEMICALLY BONDED ION-EXCHANGE STATIONARY PHASES .2. WEAK AND STRONG CATION EXCHANGERS [J].
ASMUS, PA ;
LOW, CE ;
NOVOTNY, M .
JOURNAL OF CHROMATOGRAPHY, 1976, 123 (01) :109-118
[2]   PREPARATION AND CHROMATOGRAPHIC EVALUATION OF CHEMICALLY BONDED ION-EXCHANGE STATIONARY PHASES [J].
ASMUS, PA ;
LOW, CE ;
NOVOTNY, M .
JOURNAL OF CHROMATOGRAPHY, 1976, 119 (APR28) :25-32
[3]   ON-COLUMN PREPARATION OF BONDED PHASES FOR HIGH-PRESSURE LIQUID-CHROMATOGRAPHY [J].
GILPIN, RK ;
KORPI, JA ;
JANICKI, CA .
ANALYTICAL CHEMISTRY, 1974, 46 (09) :1314-1316
[4]   SEPARATION EFFICIENCY VERSUS COLUMN LENGTH . AN EXPERIMENTAL STUDY WITH CAPILLARY COLUMNS [J].
GROB, K ;
GROB, G .
JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1969, 7 (08) :515-&
[5]  
HIRATA Y, J CHROMATOGR
[6]   STUDY OF MICRO-HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY .1. DEVELOPMENT OF TECHNIQUE FOR MINIATURIZATION OF HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].
ISHII, D ;
ASAI, K ;
HIBI, K ;
JONOKUCHI, T ;
NAGAYA, M .
JOURNAL OF CHROMATOGRAPHY, 1977, 144 (02) :157-168
[7]  
ISHII D, 1977, PITTSBURGH C ANAL CH
[8]   PERFORMANCE AND SELECTED APPLICATIONS OF A NEW RANGE OF CHEMICALLY BONDED PACKING MATERIALS IN HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].
KNOX, JH ;
PRYDE, A .
JOURNAL OF CHROMATOGRAPHY, 1975, 112 (OCT29) :171-188
[9]   PACKED MICROCAPILLARY COLUMNS IN HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].
TSUDA, T ;
NOVOTNY, M .
ANALYTICAL CHEMISTRY, 1978, 50 (02) :271-275
[10]   STUDIES OF OPEN-TUBULAR MICROCAPILLARY LIQUID-CHROMATOGRAPHY .2. CHEMICALLY BONDED OCTADECYLSILANE STATIONARY PHASE [J].
TSUDA, T ;
HIBI, K ;
NAKANISHI, T ;
TAKEUCHI, T ;
ISHII, D .
JOURNAL OF CHROMATOGRAPHY, 1978, 158 (OCT) :227-232