LIQUID-CHROMATOGRAPHIC SEPARATION OF ISOMERIC PHENANTHROLS ON MONOMERIC AND POLYMERIC C18 COLUMNS

被引：13

作者：

BAO, ZP

YANG, SK

机构：

[1] Department of Pharmacology, F. Edward Hébert School of Medicine, Uniformed Services University of the Health Sciences, Bethesda

来源：

JOURNAL OF CHROMATOGRAPHY | 1991年 / 536卷 / 1-2期

关键词：

D O I：

10.1016/S0021-9673(01)89256-6

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Separations of all five possible isomeric phenanthrols by reversed-phase high-performance liquid chromatography using a monomeric Zorbax C18 column and a polymeric Vydac C18 column were compared. With identical elution solvents and flow-rates, the phenanthrols were separated with shorter retention times on the latter column. The elution orders of the phenanthrols were different on the two columns. Ultraviolet absorption spectral properties of the phenanthrols in methanol and in alkaline methanol are reported.

引用

页码：245 / 249

页数：5

共 5 条

[1] STUDIES ON HEPATIC MICROSOMAL METABOLISM OF [PHENANTHRENE-C-14
CHATURAPIT, S
HOLDER, GM
[J]. BIOCHEMICAL PHARMACOLOGY, 1978, 27 (14) : 1865 - 1871
[2] DIHYDRODIOLS FROM ANTHRACENE AND PHENANTHRENE
JERINA, DM
SELANDER, H
YAGI, H
WELLS, MC
DAVEY, JF
MAHADEVAN, V
GIBSON, DT
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1976, 98 (19) : 5988 - 5996
[3] REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC SEPARATION OF PHENOLIC DERIVATIVES OF BENZO[A]PYRENE, BENZ[A]ANTHRACENE, AND CHRYSENE WITH MONOMERIC AND POLYMERIC C-18 COLUMNS
MUSHTAQ, M
BAO, Z
YANG, SK
[J]. JOURNAL OF CHROMATOGRAPHY, 1987, 385 : 293 - 298
[4] NORDQVIST M, 1981, MOL PHARMACOL, V19, P168
[5] Sims P, 1974, Adv Cancer Res, V20, P165, DOI 10.1016/S0065-230X(08)60111-6

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