MICROWAVE SYNTHESIS OF THE COLLOIDAL POLY(N-ISOPROPYLACRYLAMIDE) MICROGEL SYSTEM

被引：44

作者：

MURRAY, M ^{[1
]}

CHARLESWORTH, D ^{[1
]}

SWIRES, L ^{[1
]}

RIBY, P ^{[1
]}

COOK, J ^{[1
]}

CHOWDHRY, BZ ^{[1
]}

SNOWDEN, MJ ^{[1
]}

机构：

[1] UNIV GREENWICH,SCH BIOL & CHEM SCI,LONDON SE18 6PF,ENGLAND

来源：

JOURNAL OF THE CHEMICAL SOCIETY-FARADAY TRANSACTIONS | 1994年 / 90卷 / 13期

关键词：

D O I：

10.1039/ft9949001999

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

The preparation of monodisperse colloidal microgel particles of poly(N-isopropylacrylamide) by the use of microwave radiation is reported. The total synthesis time has been reduced from 6 h (conventional method) to less than 1 h (microwave method). The physicochemical characteristics of the microwave synthesized microgel are similar to those of conventionally prepared samples. This is the first report of the synthesis of a particulate colloid using microwave energy.

引用

页码：1999 / 2000

页数：2

共 12 条

[1]

[Anonymous], 1988, INTRO MICROWAVE SAMP

[2] VISIBILITY PROBLEMS FOR POLYHEDRAL TERRAINS [J].

COLE, R ;

SHARIR, M .

JOURNAL OF SYMBOLIC COMPUTATION, 1989, 7 (01) :11-30

[3]

Flory P. J., 1953, PRINCIPLES POLYM CHE

[4] THE USE OF MICROWAVE-OVENS FOR RAPID ORGANIC-SYNTHESIS [J].

GEDYE, R ;

SMITH, F ;

WESTAWAY, K ;

ALI, H ;

BALDISERA, L ;

LABERGE, L ;

ROUSELL, J .

TETRAHEDRON LETTERS, 1986, 27 (03) :279-282

[5] POLYURETHANE CURING BY A PULSED MICROWAVE FIELD [J].

JULLIEN, H ;

VALOT, H .

POLYMER, 1985, 26 (04) :506-510

[6] PREPARATION OF AQUEOUS LATTICES WITH N-ISOPROPYLACRYLAMIDE [J].

PELTON, RH ;

CHIBANTE, P .

COLLOIDS AND SURFACES, 1986, 20 (03) :247-256

[7] USE OF COLLOIDAL MICROGELS FOR THE ABSORPTION OF HEAVY-METAL AND OTHER IONS FROM AQUEOUS-SOLUTION [J].

SNOWDEN, MJ ;

THOMAS, D ;

VINCENT, B .

ANALYST, 1993, 118 (11) :1367-1369

[8]

SNOWDEN MJ, 1992, J CHEM SOC CHEM COMM, V16, P1103

[9]

SNOWDEN MJ, 1992, J CHEM SOC CHEM 0601, P803

[10]

SNOWDEN MJ, 1994, IN PRESS COLLIDS SUR

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