EPOXY MODIFIED SILICAS FOR HPLC STUDIED BY SI-29 AND C-13 SOLID-STATE NMR

被引：7

作者：

TUEL, A

HOMMEL, H

LEGRAND, AP

GONNORD, MF

MINCSOVICS, E

SIOUFFI, AM

机构：

[1] ECOLE SUPER PHYS & CHIM IND,PHYS QUANT LAB,UA 421,10 RUE VAUQUELIN,F-75231 PARIS 05,FRANCE

[2] LAB MIM TUZOLTO,H-2000 BUDAPEST,HUNGARY

[3] LAB GENIE CHIM & CHIM APPL,F-13397 MARSEILLE,FRANCE

[4] ECOLE POLYTECH,DCMR,F-91128 PALAISEAU,FRANCE

来源：

JOURNAL DE CHIMIE PHYSIQUE ET DE PHYSICO-CHIMIE BIOLOGIQUE | 1992年 / 89卷 / 02期

关键词：

D O I：

10.1051/jcp/1992890477

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

Epoxy monomer and polymer chains have been prepared on a silica substrate. In all cases in addition to the awaited reaction a zip-polymerisation of the grafts along the silica surface occurs. In the monomer sample there exist some simple grafts without lateral chemical reactions but they are neither the only ones neither the most abundant.

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页码：477 / 488

页数：12

相关论文

共 21 条

[1] LIQUID-CHROMATOGRAPHY OF SUGARS ON DIOL COLUMNS - DETECTION WITH CUPRAMMONIUM REAGENT [J].

ABBOU, M ;

SIOUFFI, AM .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1987, 10 (01) :95-106

[2] A NUCLEAR MAGNETIC RESONANCE INVESTIGATION OF SOLID CYCLOHEXANE [J].

ANDREW, ER ;

EADES, RG .

PROCEEDINGS OF THE ROYAL SOCIETY OF LONDON SERIES A-MATHEMATICAL AND PHYSICAL SCIENCES, 1953, 216 (1126) :398-412

[3] CHARACTERIZATION OF CHEMICALLY MODIFIED SILICA-GELS BY SI-29 AND C-13 CROSS-POLARIZATION AND MAGIC ANGLE SPINNING NUCLEAR MAGNETIC-RESONANCE [J].

BAYER, E ;

ALBERT, K ;

REINERS, J ;

NIEDER, M ;

MULLER, D .

JOURNAL OF CHROMATOGRAPHY, 1983, 264 (02) :197-213

[4] THEORY OF LINE NARROWING BY DOUBLE-FREQUENCY IRRADIATION [J].

BLOCH, F .

PHYSICAL REVIEW, 1958, 111 (03) :841-853

[5]

ENGELHARDT H, 1987, J LIQ CHROMATOGR, V10, P199

[6] DIPOLAR SPIN FLUCTUATIONS IN THE ROTATING FRAME - RELAXATION MECHANISM [J].

GARROWAY, AN .

JOURNAL OF MAGNETIC RESONANCE, 1979, 34 (02) :283-293

[7]

GARROWAY AN, 1979, ARC S SER, V103, P509

[8] THE SIZE-EXCLUSION CHROMATOGRAPHIC BEHAVIOR OF SYNTHETIC WATER-SOLUBLE POLYMERS ON DIOL BONDED PHASE SUPPORTS [J].

HERMAN, DP ;

FIELD, LR ;

ABBOTT, S .

JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1981, 19 (09) :470-476

[9] STUDY OF THE CHANGES IN MONOFUNCTIONAL, DIFUNCTIONAL AND TRIFUNCTIONAL OCTADECYL-MODIFIED PACKINGS FOR REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY WITH DIFFERENT ELUENT COMPOSITIONS [J].

HETEM, M ;

VANDEVEN, L ;

DEHAAN, J ;

CRAMERS, C .

JOURNAL OF CHROMATOGRAPHY, 1989, 479 (02) :269-295

[10]

Iler R., 1979, CHEM SILICA