THE DETERMINATION OF NITRATE AND NITRITE IN CURED MEAT BY HPLC/UV

被引:41
作者
DENNIS, MJ
KEY, PE
PAPWORTH, T
POINTER, M
MASSEY, RC
机构
[1] Ministry of Agriculture, Fisheries and Food, Food Science Division
[2] School of Chemistry, Thames Polytechnic
来源
FOOD ADDITIVES AND CONTAMINANTS | 1990年 / 7卷 / 04期
关键词
Cured meats; HPLC; Nitrate; Nitrite;
D O I
10.1080/02652039009373908
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
A rapid strong anion exchange HPLC/UV procedure has been developed for the determination of nitrate and nitrite in a wide variety of cured meats. The accuracy of this technique has been confirmed by the good agreement achieved with the existing British Standard colorimetric method. The applicability and repeatability of the procedure has been established in a survey of over 200 samples. The agreement between duplicate determinations and their respective means averaged ±3.4% for nitrite and ±4.3% for nitrate as defined by the term [(a - b)/(a + b)] x 100% where a and b are the repeat determination values. © 1990 Taylor & Francis Ltd.
引用
收藏
页码:455 / 461
页数:7
相关论文
共 15 条
  • [1] Meat and meat products, Part 7, determination of nitrate content. Part 8, determination of nitrite content, (1976)
  • [2] Cassens R.G., Woolford G., Lee S.H., Goutefongea R., Fate of nitrite in meat, Proceedings of the Second International Symposium on Nitrite in Meat Products, pp. 95-100, (1977)
  • [3] Eggers N.J., Cattle D.L., High-performance liquid chromatographic method for the determination of nitrate and nitrite in cured meat, Journal of Chromatography, 354, pp. 490-494, (1986)
  • [4] Giddings G.C., The basis of color in muscle food, Critical Reviews in Food Science and Nutrition, 5, pp. 81-114, (1977)
  • [5] Hunt J., Seymour D.H., Method for measuring nitrate-nitrogen in vegetables using anion-exchange high-performance liquid chromatography, Analyst, 110, pp. 131-133, (1985)
  • [6] Jackson P.E., Haddad P.R., Dilli S., Determination of nitrate and nitrite in cured meats using high-performance liquid chromatography, 295, pp. 471-478, (1984)
  • [7] Nitrate, Nitrite and N-Nitroso Compounds in Food, First Supplementary Report, Food Surveillance Paper, (1990)
  • [8] Olsman W.J., Chemical behaviour of nitrite in meat products. 1. The stability of protein bound nitrite during storage, Proceedings of the Second International Symposium on Nitrite in Meat Products, pp. 101-110, (1977)
  • [9] Olsman W.J., Leeuwen V., The assay of protein-bound nitrite in meat products, Zeitschrift Für Lebensmittel‐Untersuchung Und ‐Forschung, 164, pp. 239-242, (1977)
  • [10] Paquette M., Robach W.M., Sofos C., Busta F.F., Effects of various concentrations of sodium nitrite and potassium sorbate on color and sensory qualities of commercially prepared bacon, Journal of Food Science, 45, pp. 1293-1296, (1980)