FLAME IONIZATION DETECTION RELATIVE RESPONSE FACTORS OF SOME POLYCYCLIC AROMATIC-COMPOUNDS - DETERMINATION OF THE MAIN COMPONENTS OF THE COAL-TAR PITCH VOLATILE FRACTION

被引：37

作者：

BLANCO, CG ^{[1
]}

CANGA, JS ^{[1
]}

DOMINGUEZ, A ^{[1
]}

IGLESIAS, MJ ^{[1
]}

GUILLEN, MD ^{[1
]}

机构：

[1] UNIV BASQUE COUNTRY, FAC FARM, E-01007 VITORIA, SPAIN

来源：

JOURNAL OF CHROMATOGRAPHY | 1992年 / 607卷 / 02期

关键词：

D O I：

10.1016/0021-9673(92)87088-P

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The flame ionization detection (FID) relative response factors of some commercially available polycyclic aromatic compounds using split injection were determined and compared with other published FID relative response factors obtained using splitless and cold on-column injection technique. From these data FID relative response factors of some non-available polycyclic aromatic compounds were calculated in an approximate way. These factors were used in a quantitative study of the main components of a coal tar pitch volatile fraction. For this quantification the internal standard method and the absolute calibration with separate standard method were employed. Good reproducibility of the determinations using both methods was found.

引用

页码：295 / 302

页数：8

共 21 条

[1] FACTORS AFFECTING THE RETENTION OF POLYCYCLIC AROMATIC-HYDROCARBONS IN GAS-CHROMATOGRAPHY [J].