INVESTIGATIONS OF A DIOL-BASED SOL-GEL PROCESS FOR THE PREPARATION OF LEAD TITANATE MATERIALS

被引：66

作者：

CALZADA, ML

SIRERA, R

CARMONA, F

JIMENEZ, B

机构：

[1] Instituto de Ciencia de Materiales de Madrid, Madrid

来源：

JOURNAL OF THE AMERICAN CERAMIC SOCIETY | 1995年 / 78卷 / 07期

关键词：

D O I：

10.1111/j.1151-2916.1995.tb08892.x

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Lead titanate sols were prepared by a sol-gel method from lead acetate trihydrate, Pb(OOCCH3)(2) . 3H(2)O, and titanium di-isopropoxide bis-acetylacetonate, Ti (OC3H7)(2)-(CH3COCHCOCH3)(2), in 1,3-propanediol, HO(CH2)(3)OH, as solvent. IR analysis and NMR spectroscopic techniques were used to study the reaction mechanisms and to identify possible polymer structures developed during synthesis of the solutions.

引用

页码：1802 / 1808

页数：7

共 30 条

[1] ACETATES AND ACETATO-COMPLEXES .2. SPECTROSCOPIC STUDIES
ALCOCK, NW
TRACY, VM
WADDINGTON, TC
[J]. JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1976, (21): : 2243 - 2246
[2] SOL-GEL-DERIVED PBTIO3
BLUM, JB
GURKOVICH, SR
[J]. JOURNAL OF MATERIALS SCIENCE, 1985, 20 (12) : 4479 - 4483
[3] BRADLEY DC, 1987, METAL ALKOXIDES, P183
[4] BRINKER CJ, 1990, SOL GEL SCI PHYS CHE, P617
[5] Budd K.D., 1986, MATER RES SOC S P, V73, P711
[6] Calzada M. L., 1994, Ferroelectrics, V152, P19, DOI 10.1080/00150199408017590
[7] CALZADA ML, 1993, J MATER SCI LETT, V12, P1221
[8] THE ROLE OF DRYING-CONTROL CHEMICAL ADDITIVES ON THE PREPARATION OF SOL-GEL DERIVED PLZT THIN-FILMS
CHANG, DA
CHOH, YH
HSIEH, WF
LIN, P
TSENG, TY
[J]. JOURNAL OF MATERIALS SCIENCE, 1993, 28 (24) : 6691 - 6698
[9] CHEWASATN S, 1993, 3RD EUROCERAMICS, V1, P335
[10] DEKLEWA TW, 1988, J AM CERAM SOC, V7, pC280

← 1 2 3 →