IMPROVEMENTS TO METHOD PERFORMANCE FOR ENVIRONMENTAL MONITORING OF DIOXINS AND DIBENZOFURANS

被引:5
作者
DONNELLY, JR
MUNSLOW, WD
NUNN, NJ
GRANGE, AH
VONNAHME, TL
FISK, JF
SOVOCOOL, GW
机构
[1] US EPA, LAS VEGAS, NV 89193 USA
[2] US EPA, WASHINGTON, DC 20460 USA
关键词
D O I
10.1016/0045-6535(90)90092-8
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
Relative efficiencies of various sample preparation techniques were measured for analysis of chlorinated dioxins and dibenzofurans (PCDD, PCDF) in representative wastes. The following sample cleanup columns were tested: a mixed phase column of acid, base, and neutral silica; neutral and acidic alumina columns; Carbopack/Celite and AX-21 carbon adsorption columns. Chlorinated dioxins and dibenzofurans were analyzed in fly ash, still bottom, fuel oil, and sludge matrices for this study. The multi-phase silica, acidic alumina, and AX-21 columns were determined to be the most suitable combination for PCDD and PCDF analytes. © 1990.
引用
收藏
页码:123 / 136
页数:14
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