STRUCTURE OF N-METHYL BENZALDEHYDE NITRONE

被引:12
作者
BEDFORD, RB [1 ]
CHALONER, PA [1 ]
HITCHCOCK, PB [1 ]
机构
[1] UNIV SUSSEX,SCH CHEM & MOLEC SCI,BRIGHTON BN1 9RH,E SUSSEX,ENGLAND
关键词
D O I
10.1107/S0108270191007199
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
N-(Benzylidene)methylamine N-oxide, C8H9NO, M(r) = 135.2, orthorhombic, Pbca, a = 9.665 (2), b = 7.981 (1), c = 19.071 (2) angstrom, U = 1471.0 angstrom 3, Z = 8, D(x) = 1.22 g cm-3, lambda(Mo K-alpha) = 0.71069 angstrom, mu = 0.8 cm-1, F(000) = 576, T = 298 K, R = 0.043 and wR = 0.050 for 661 observed reflections with \F2\ > 3-sigma(F2). The geometry about the carbon-nitrogen double bond is Z, and there is little deviation from planarity.
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页码:2484 / 2485
页数:2
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