REDETERMINATION OF TETRAPHENYLLEAD

被引：16

作者：

PREUT, H

HUBER, F

机构：

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1993年 / 49卷

关键词：

D O I：

10.1107/S0108270193001878

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The redetermination with diffractometer data corroborates the results of a prior study [Busetti, Mammi, Signor & del Pra (1967). Inorg. Chim. Acta, 1, 424-428] which was performed on the basis of 70 observed (hk0) and 38 observed (h0l) film reflections recorded with a microdensitometer. The bonding sphere around Pb in (C6H5)4Pb is practically a regular tetrahedron with a maximum deviation of 0.8-degrees from the ideal angle and a mean value of 109.5 (2)-degrees.

引用

页码：1372 / 1373

页数：2

共 13 条

[1]

Busetti V., 1967, INORG CHIM ACTA, V1, P424

[2] TETRA-PARA-TOLYL COMPOUNDS PARA-TOL4SI AND PARA-TOL4GE - CONFIGURATION OF TETRARYL METHANEANALOGS AR4M (M = C,SI,GE,SN,PB) [J].