A RAPID ASSAY FOR THE DETERMINATION OF SARAFLOXACIN (A-55620) IN FISH SERUM BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
被引:11
作者:
STEFFENAK, I
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机构:Department of Food Hygiene, Norwegian College of Veterinary Medicine, N-0033 Oslo 1
STEFFENAK, I
HORMAZABAL, V
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机构:Department of Food Hygiene, Norwegian College of Veterinary Medicine, N-0033 Oslo 1
HORMAZABAL, V
YNDESTAD, M
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机构:Department of Food Hygiene, Norwegian College of Veterinary Medicine, N-0033 Oslo 1
YNDESTAD, M
机构:
[1] Department of Food Hygiene, Norwegian College of Veterinary Medicine, N-0033 Oslo 1
来源:
JOURNAL OF LIQUID CHROMATOGRAPHY
|
1991年
/
14卷
/
10期
关键词:
D O I:
10.1080/01483919108049668
中图分类号:
Q5 [生物化学];
学科分类号:
071010 ;
081704 ;
摘要:
A simple, rapid, and sensitive method for the determination of sarafloxacin (A-55620) in fish serum using enrofloxacin as internal standard is described. The serum sample and internal standard enrofloxacin are loaded onto the extraction column packed with C2 sorbent material. The column is rinsed and then eluted. The detection limit is 5 ng/g, the recovery rate varying from 92 to 100 %.