共 3 条
A MACROCYCLIC AMIDE FROM DEHYDROCHLORINATION OF INDOLE-3-CARBONYL CHLORIDE
被引:5
作者:
OLIVER, JE
[1
]
WATERS, RM
[1
]
LUSBY, WR
[1
]
FLIPPENANDERSON, JL
[1
]
机构:
[1] USN,RES LAB,STRUCT MATTER LAB,WASHINGTON,DC 20375
关键词:
D O I:
10.1002/jhet.5570280619
中图分类号:
O62 [有机化学];
学科分类号:
070303 ;
081704 ;
摘要:
Indolyl-3-ketene 3 was generated from two precursors and was found to form a symmetrical tetramer 4 consisting of a sixteen-membered ring amide. The tetramer was characterized by mass spectrometry, infrared, H-1 and C-13-nmr spectroscopy, and single crystal X-ray crystallography.
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页码:1569 / 1572
页数:4
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