GAS-CHROMATOGRAPHIC DETERMINATION OF PHENOLS IN AQUEOUS SAMPLES AFTER SOLID-PHASE EXTRACTION

被引：56

作者：

MUSSMANN, P

LEVSEN, K

RADECK, W

机构：

[1] FRAUNHOFER INST TOXICOL & AEROSOL RES,NIKOLAI FUCHS STR 1,D-30625 HANNOVER,GERMANY

[2] RHEIN WESTFAL TECH UBERWACHUNGSVEREIN,D-45141 ESSEN,GERMANY

来源：

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1994年 / 348卷 / 10期

关键词：

D O I：

10.1007/BF00325568

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

27 phenols including mono-, di-, tri-, tetra- and pentachlorophenols, mono- and dinitrophenols, mono- and dinitrocresols and dimethylnitrophenols have been extracted from aqueous samples by solid phase extraction using both modified silica gel (C18) and XAD resin-adsorbents and determined by gas chromatography (GC) using capillary columns with specially desactivated weakly polar phases. If a 11 sample of spiked water is used, a considerable breakthrough is observed with phenol itself, while all other phenols are almost quantitatively extracted. The recovery of phenol itself can be improved by employing smaller sample volumes.

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页码：654 / 659

页数：6

相关论文

共 36 条

[1] DETERMINATION OF NITROPHENOLS IN RAIN AND SNOW [J].

ALBER, M ;

BOHM, HB ;

BRODESSER, J ;

FELTES, J ;

LEYSEN, K ;

SCHOLER, HF .

FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 1989, 334 (06) :540-545

[2] DIRECT-INJECTION GLC ANALYSIS OF XYLENOLS IN INDUSTRIAL WASTEWATERS [J].

BAIRD, RB ;

CARMONA, LG ;

JENKINS, RL .

BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY, 1977, 17 (06) :764-767

[3] A GAS-CHROMATOGRAPHIC MICROMETHOD FOR TRACE DETERMINATIONS OF PHENOLS [J].

BENGTSSON, G .

JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1985, 23 (09) :397-401

[4] DETERMINATION OF PHENOLS IN WATER AND WASTE-WATER BY POSTCOLUMN REACTION DETECTION HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].

BIGLEY, FP ;

GROB, RL .

JOURNAL OF CHROMATOGRAPHY, 1985, 350 (02) :407-416

[5]

BOHM HB, 1989, J CHROMATOGR, V478, P399

[6] EVALUATION OF GRAPHITIZED CARBON-BLACK CARTRIDGES FOR RAPID ORGANIC TRACE ENRICHMENT FROM WATER - APPLICATION TO PRIORITY POLLUTANT PHENOLS [J].

BORRA, C ;

DICORCIA, A ;

MARCHETTI, M ;

SAMPERI, R .

ANALYTICAL CHEMISTRY, 1986, 58 (09) :2048-2052

[7] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF 4-NITROSOPHENOLS AND 4-NITROPHENOLS IN THE PRESENCE OF PHENOL AND ALKYLPHENOLS [J].

BORYS, A .

JOURNAL OF CHROMATOGRAPHY, 1981, 216 (OCT) :361-366

[8] GAS-CHROMATOGRAPHIC ANALYSIS OF TRACE PHENOLS BY DIRECT ACETYLATION IN AQUEOUS-SOLUTION [J].

COUTTS, RT ;

HARGESHEIMER, EE ;

PASUTTO, FM .

JOURNAL OF CHROMATOGRAPHY, 1979, 179 (02) :291-299

[9] DETERMINATION OF TRACE LEVELS OF PHENOL AND CRESOLS IN RAIN BY CONTINUOUS LIQUID-LIQUID-EXTRACTION AND HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY [J].

CZUCZWA, J ;

LEUENBERGER, C ;

TREMP, J ;

GIGER, W ;

AHEL, M .

JOURNAL OF CHROMATOGRAPHY, 1987, 403 :233-241

[10]

DUNLAP WJ, 1976, IDENTIFICATION ANAL, P453

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