PROCESSING OF SILICA XEROGELS USING SONOCATALYSIS AND AN ADDITIVE

被引:13
作者
BLANCO, E
DELAROSAFOX, N
ESQUIVIAS, L
CRAIEVICH, AF
机构
[1] LAB NACL LUZ SINCROTRON,CNPA,CAMPINAS,SP,BRAZIL
[2] UNIV SAO PAULO,INST FIS,SAO PAULO,BRAZIL
关键词
D O I
10.1016/S0022-3093(05)80633-7
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Drying control chemical additives (DCCA) can be used to obtain monolithic glasses. Processing steps are unclear or not well known. This work studies the processing of xerogels prepared with formamide as an additive, tetraethoxysilane (TEOS) and acid water in a molar ratio of 7:1:10, respectively, with high power ultrasound. In order to calculate the evolution of the main ultrastructural parameters, the entire processing has been followed by small-angle X-ray scattering (SAXS) and nitrogen adsorption-desorption isotherms.
引用
收藏
页码:296 / 302
页数:7
相关论文
共 19 条
[1]   SORPTION OF NITROGEN IN POROUS COMPACTS OF SILICA AND ZIRCONIA POWDERS [J].
AVERY, RG ;
RAMSAY, JDF .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 1973, 42 (03) :597-606
[2]  
de la Rosa-Fox N., 1987, Diffusion and Defect Data, V53-54, P363
[3]   SILICA SONOGELS WITH DRYING CONTROL CHEMICAL ADDITIVES [J].
DELAROSAFOX, N ;
ESQUIVIAS, L .
JOURNAL OF MATERIALS SCIENCE LETTERS, 1991, 10 (21) :1237-1242
[4]  
DELAROSAFOX N, IN PRESS
[5]  
DELAROSAFOX N, 1987, DIFF DEFECT DATA, V54, P363
[6]  
Fricke J., 1987, AEROGELS
[7]   GEL-GLASS TRANSFORMATION IN THE SIO2-FE2O3 SYSTEM [J].
GUGLIELMI, M ;
PRINCIPI, G .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 1982, 48 (01) :161-175
[8]  
HENCH LL, 1986, SCI CERAMIC CHEM PRO, P52
[9]  
Kennedy J. C., 1964, PHYS CHEM GLASSES-B, V5, P130
[10]   STRUCTURAL EVOLUTION AT LOW-TEMPERATURE OF FORMAMIDE MODIFIED SILICA XEROGELS [J].
ORCEL, G ;
PHALIPPOU, J ;
HENCH, L .
JOURNAL OF NON-CRYSTALLINE SOLIDS, 1988, 104 (2-3) :170-180