QUANTIFICATION OF VOLATILE SOLVENTS IN BLOOD BY STATIC HEADSPACE ANALYSIS

被引:20
作者
DILLS, RL
KENT, SD
CHECKOWAY, H
KALMAN, DA
机构
[1] Department of Environmental Health, School of Public Health and Community Medicine, University of Washington, Seattle
关键词
D O I
10.1016/0039-9140(91)80073-9
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A static headspace method for determination of volatile solvents in blood was developed. The solvents determined were 1,1,1-trichloroethane, toluene, xylene (o-, m- and p-), ethylbenzene, styrene, alpha-methylstyrene and 4-methylstyrene at concentrations ranging from 0.01 to 1-mu-g/ml. Internal standard calibration was used. Parameters affecting sensitivity and precision were determined and optimized.
引用
收藏
页码:365 / 374
页数:10
相关论文
共 23 条
[1]  
CHRISTMORE DS, 1984, J FORENSIC SCI, V29, P1038
[2]   DISTRIBUTION OF TRICHLOROETHYLENE BETWEEN PLASMA AND ERYTHROCYTES IN WHOLE-BLOOD FROM FASTING SUBJECTS [J].
DAVIES, DD ;
DOUGLAS, RB ;
LING, S .
BRITISH JOURNAL OF ANAESTHESIA, 1986, 58 (12) :1440-1442
[3]   SAMPLE HANDLING AND STORAGE FOR THE QUANTITATIVE-ANALYSIS OF VOLATILE COMPOUNDS IN BLOOD - THE DETERMINATION OF TOLUENE BY HEADSPACE GAS-CHROMATOGRAPHY [J].
GILL, R ;
HATCHETT, SE ;
OSSELTON, MD ;
WILSON, HK ;
RAMSEY, JD .
JOURNAL OF ANALYTICAL TOXICOLOGY, 1988, 12 (03) :141-146
[4]  
IOFFE BV, 1982, HEADSPACE ANAL RELAT
[5]  
JAKUBOWSKI M, 1980, BROMATOL CHEM TOKSYK, V13, P263
[6]  
JANSEN LJ, 1987, THESIS U WASHINGTON
[7]  
KAMLET MJ, 1986, CHEMTECH, V16, P566
[8]  
KERSTING H, 1986, Zeitschrift fuer die Gesamte Hygiene und ihre Grenzgebiete, V32, P552
[9]   CRYOFOCUSING IN THE COMBINATION OF GAS-CHROMATOGRAPHY WITH EQUILIBRIUM HEADSPACE SAMPLING [J].
KOLB, B ;
LIEBHARDT, B ;
ETTRE, LS .
CHROMATOGRAPHIA, 1986, 21 (06) :305-311
[10]   HEADSPACE DETERMINATION OF SOLUBILITY LIMITS OF THE BASE NEUTRAL AND VOLATILE COMPONENTS FROM THE ENVIRONMENTAL-PROTECTION-AGENCYS LIST OF PRIORITY POLLUTANTS [J].
MCNALLY, ME ;
GROB, RL .
JOURNAL OF CHROMATOGRAPHY, 1984, 284 (01) :105-116