RESIDUAL LINEWIDTHS OF NMR-SPECTRA OF SPIN-1/2 SYSTEMS UNDER MAGIC-ANGLE SPINNING

被引：70

作者：

BRUNNER, E

FREUDE, D

GERSTEIN, BC

PFEIFER, H

机构：

[1] IOWA STATE UNIV,DEPT CHEM,AMES,IA 50010

[2] US DOE,AMES LAB,AMES,IA 50010

来源：

JOURNAL OF MAGNETIC RESONANCE | 1990年 / 90卷 / 01期

关键词：

D O I：

10.1016/0022-2364(90)90367-I

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The residual linewidths of NMR spectra of spin- 1 2 systems in solids under magic-angle spinning conditions are calculated in the rigid lattice limit for the general case where both homo- and heteronuclear dipolar interactions as well as shielding anisotropy may be present. The results are used to quantitatively interpret 1H MAS NMR spectra of crystalline water in gypsum and of hydroxyl groups in zeolites. © 1990.

引用

页码：90 / 99

页数：10

共 13 条

[1] EFFECTS OF QUADRUPOLAR NUCLEI ON NMR-SPECTRA OF I=1/2 NUCLEI IN MAGIC-ANGLE SPINNING EXPERIMENTS
BOHM, J
FENZKE, D
PFEIFER, H
[J]. JOURNAL OF MAGNETIC RESONANCE, 1983, 55 (02) : 197 - 204
[2] BRUNNER E, 1989, THESIS KARL MARX U L
[3] THEORETICAL STUDIES OF MAGNETIC SHIELDING IN H2O AND (H2O)2
DITCHFIELD, R
[J]. JOURNAL OF CHEMICAL PHYSICS, 1976, 65 (08) : 3123 - 3133
[4] SOLID-STATE NMR-STUDIES OF THE GEOMETRY OF BRONSTED ACID SITES IN ZEOLITIC CATALYSTS
FREUDE, D
KLINOWSKI, J
HAMDAN, H
[J]. CHEMICAL PHYSICS LETTERS, 1988, 149 (04) : 355 - 362
[5] INVESTIGATION OF ACIDIC PROPERTIES OF ZEOLITES BY MAS NMR
FREUDE, D
HUNGER, M
PFEIFER, H
[J]. ZEITSCHRIFT FUR PHYSIKALISCHE CHEMIE NEUE FOLGE, 1987, 152 : 171 - 182
[6] HIGH-RESOLUTION NMR SPECTROMETRY OF SOLIDS .2.
GERSTEIN, BC
[J]. ANALYTICAL CHEMISTRY, 1983, 55 (08) : A899 - &
[7] GERSTEIN BC, 1983, ANAL CHEM, V5, pA781
[8] GERSTEIN BC, 1985, TRANSIENT TECHNIQUES, pCH5
[9] GERSTEIN BC, 1985, TRANSIENT TECHNQIUES, pCH4
[10] HIGH-RESOLUTION PROTON NMR-STUDY OF GYPSUM, CASO4.2H2O
MCKNETT, CL
DYBOWSKI, CR
VAUGHAN, RW
[J]. JOURNAL OF CHEMICAL PHYSICS, 1975, 63 (11) : 4578 - 4581

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