SPECIFIC DEUTERATION EFFECTS ON C-13 NMR RELAXATION DATA OF AMIDO-TYPE SYSTEMS

被引：10

作者：

SHAPIRO, MJ

KAHLE, AD

机构：

[1] Pharmaceutical Research and Development, Sandoz, Inc., East Hanover, New Jersey

来源：

ORGANIC MAGNETIC RESONANCE | 1979年 / 12卷 / 04期

关键词：

D O I：

10.1002/mrc.1270120413

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The effect of deuterium substitution in amido‐systems is explored. For benzamide, both positive and negative changes in TDD1 are observed. A method for structure elucidation of these and related systems is presented. Copyright © 1979 Heyden & Son Ltd.

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页码：235 / 236

页数：2

相关论文

共 12 条

[1]

BARCZA S, UNPUBLISHED

[2] SPECTROSCOPIC STUDIES OF KETO-ENOL EQUILIBRIA .7. NITROGEN-15 SUBSTITUTED SCHIFF BASES [J].

DUDEK, GO ;

DUDEK, EP .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1964, 86 (20) :4283-&

[3] C-13 NUCLEAR MAGNETIC-RESONANCE SPECTRAL ANALYSIS USING SPIN-LATTICE RELAXATION DATA AND SPECIFIC DEUTERATION - THIAMINE HYDROCHLORIDE [J].

ECHOLS, RE ;

LEVY, GC .

JOURNAL OF ORGANIC CHEMISTRY, 1974, 39 (09) :1321-1322

[4] ASSIGNMENT OF C-13 RESONANCES FROM CARBONYL GROUPS IN PEPTIDES [J].

FEENEY, J ;

PARTINGT.P ;

ROBERTS, GCK .

JOURNAL OF MAGNETIC RESONANCE, 1974, 13 (03) :268-274

[5] HIGH-RESOLUTION STUDIES OF NUCLEAR SPIN-LATTICE RELAXATION [J].

FREEMAN, R ;

HILL, HDW .

JOURNAL OF CHEMICAL PHYSICS, 1969, 51 (07) :3140-&

[6]

HAWKES GE, COMMUNICATION

[7] ANALYSIS OF DEUTERIOBENZONITRILES BY C-13 NUCLEAR MAGNETIC RESONANCE SPECTROMETRY [J].

LEBEL, GL ;

LAPOSA, JD ;

SAYER, BG ;

BELL, RA .

ANALYTICAL CHEMISTRY, 1971, 43 (11) :1500-&

[8] ASSIGNMENT OF PRIMARY AND SECONDARY AMIDE CARBONYL RESONANCES IN C-13 NMR [J].

NEWMARK, RA ;

HILL, JR .

JOURNAL OF MAGNETIC RESONANCE, 1976, 21 (01) :1-7

[9]

NEWMARK RA, 1977, 18TH ENC AS CAL

[10]

OZUBKO RS, CAN J