学术探索
学术期刊
新闻热点
数据分析
智能评审

DETERMINATION OF LYSERGIC-ACID DIETHYLAMIDE (LSD) IN URINE BY INSTRUMENTAL HIGH-PERFORMANCE THIN-LAYER CHROMATOGRAPHY

被引：18
作者：
BLUM, LM
CARENZO, EF
RIEDERS, F
机构：
[1] National Medical Services Inc., Willow Grove, PA, 19090
来源：
JOURNAL OF ANALYTICAL TOXICOLOGY | 1990年 / 14卷 / 05期
关键词：
D O I：
10.1093/jat/14.5.285
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
An instrumental high-performance thin-layer chromatographic (HPTLC) technique for the determination of lysergic acid diethylamide (LSD) in urine was developed. Before chromatographic separation, a single-step extraction with alkaline wash is performed. The procedure can detect less than 1 μg LSD/L urine. Results of HPTLC determination are compared with those from a radioimmunoassay (RIA) procedure. © 1990 Oxford University Press.
引用
收藏
页码：285 / 287
页数：3
相关论文
共 11 条
[1]  
CLARK CC, 1989, J FORENSIC SCI, V34, P532
[2]   IDENTIFICATION AND ESTIMATION OF LYSERGIC ACID DIETHYLAMIDE BY THIN LAYER CHROMATOGRAPHY AND FLUOROMETRY [J].
DALCORTIVO, LA ;
BROICH, JR ;
DIHRBERG, A ;
NEWMAN, B .
ANALYTICAL CHEMISTRY, 1966, 38 (13) :1959-+
[3]  
FRANCOM P, 1988, J ANAL TOXICOL, V12, P1
[4]   THIN-LAYER CHROMATOGRAPHY OF ERGOT ALKALOIDS IN PHARMACEUTICAL PREPARATIONS [J].
FRENCH, WN ;
WEHRLI, A .
JOURNAL OF PHARMACEUTICAL SCIENCES, 1965, 54 (10) :1515-&
[5]   QUANTIFICATION OF LSD AND N-DEMETHYL-LSD IN URINE BY GAS-CHROMATOGRAPHY RESONANCE ELECTRON-CAPTURE IONIZATION MASS-SPECTROMETRY [J].
LIM, HK ;
ANDRENYAK, D ;
FRANCOM, P ;
FOLTZ, RL ;
JONES, RT .
ANALYTICAL CHEMISTRY, 1988, 60 (14) :1420-1425
[6]   RADIOIMMUNOASSAY FOR LYSERGIDE (LSD) IN ILLICIT DRUGS AND BIOLOGICAL-FLUIDS [J].
LOEFFLER, LJ ;
PIERCE, JV .
JOURNAL OF PHARMACEUTICAL SCIENCES, 1973, 62 (11) :1817-1820
[7]  
MCDONALD P, 1984, J FORENSIC SCI, V29, P120
[8]  
SHERMA J, 1981, TLC TECHNICAL SERIES, V2
[9]   FATE OF LYSERGIC-ACID DIETHYLAMIDE-C-14 ([LSD-C-14) IN THE RAT, GUINEA-PIG AND RHESUS-MONKEY AND OF [ISO-LSD-C-14 IN RAT [J].
SIDDIK, ZH ;
BARNES, RD ;
DRING, LG ;
SMITH, RL ;
WILLIAMS, RT .
BIOCHEMICAL PHARMACOLOGY, 1979, 28 (20) :3093-3101
[10]   LYSERGIC-ACID DIETHYLAMIDE - RADIOIMMUNOASSAY [J].
TAUNTONRIGBY, A ;
SHER, SE ;
KELLEY, PR .
SCIENCE, 1973, 181 (4095) :165-166
12