SYNTHESIS MARKERS IN ILLEGALLY MANUFACTURED 3,4-METHYLENEDIOXYAMPHETAMINE AND 3,4-METHYLENEDIOXYMETHAMPHETAMINE

被引：26

作者：

BOHN, M ^{[1
]}

BOHN, G ^{[1
]}

BLASCHKE, G ^{[1
]}

机构：

[1] WESTFAL WILHELMS UNIV,INST PHARMAZEUT CHEM,D-48149 MUNSTER,GERMANY

来源：

INTERNATIONAL JOURNAL OF LEGAL MEDICINE | 1993年 / 106卷 / 01期

关键词：

MDA; MDMA; SYNTHESIS MARKERS; LEUCKART-WALLACH SYNTHESIS; REDUCTIVE AMINATION;

D O I：

10.1007/BF01225019

中图分类号：

DF [法律]; D9 [法律]; R [医药、卫生];

学科分类号：

0301 ; 10 ;

摘要：

In this paper the isolation and identification of 12 compounds as impurities in illicit 3,4-methylenedioxyamphetamine (MDA) and 3,4-methylenedioxymethamphetamine (MDMA) is reported. Isolation of these substances is performed by preparative TLC, while identification is performed by using mass spectrometry and H-1-NMR spectroscopy. A simple and rapid method for detection of these impurities in seized MDA and MDMA samples is described. The identification of the impurities can provide numerous points on which to base comparative analysis of different exhibits.

引用

页码：19 / 23

页数：5

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