STRUCTURE OF BIS(P-METHOXYPHENYLTELLURO)ETHYNE

被引:6
作者
DEMATHEUS, M [1 ]
TORRES, L [1 ]
CABIATIVA, C [1 ]
FUERTES, A [1 ]
MIRAVITLLES, C [1 ]
机构
[1] UNIV NACL COLOMBIA, DEPT QUIM, SANTA FE DE BOGOTA, COLOMBIA
来源
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 1991年 / 47卷
关键词
D O I
10.1107/S0108270190007570
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
C16H14O2Te2, M(r) = 493.3, monoclinic, P2(1)/n, a = 7.911 (3), b = 6.671 (6), c = 15.443 (4) angstrom, beta = 95.4 (4)degrees, V = 811.1 angstrom 3, Z = 2, D(x) = 2.02 g cm-3, Mo K-alpha, lambda = 0.70926 angstrom, mu = 36.02 cm-1, F(000) = 460, room temperature, R = 0.051, wR = 0.053 for 1429 observed reflections [I greater-than-or-equal-to 2.5-sigma(I)]. The structure is characterized by centrosymmetric binuclear molecules linked through the acetylenic moiety, with foru atoms almost linear: Te(1)-C(1)-C(1*)-Te(1*).
引用
收藏
页码:977 / 980
页数:4
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