Obtaining and Sintering Yttria Stabilized Zirconia (YSZ) Powders from Alkoxides

被引:4
作者
Barrera-Solano, C. [1 ]
Jimenez-Solis, C. [1 ]
De La Rosa-Fox, N. [1 ]
Esquivias, L. [1 ]
机构
[1] Univ Cadiz, Fac Ciencias, Dept Estruct & Propiedades Mat, Cadiz 11510, Spain
关键词
zirconia; sintering; densification; heat treatment; yttria stabilized zirconia;
D O I
10.1007/BF00486268
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Amorphous zirconia ceramics powders containing 3 and 6 mol% yttria were prepared by controlled hydrolysis of alkoxides. Characterization of these powders was carried away by Thermal Analysis, X-ray Diffraction, Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray Analysis (EDAX (TM)). The calcination temperature was optimized for compaction at a temperature ranging from 500-800 degrees C. 3% molar YSZ powders from alkoxide, that attained 98% of the theoretical bulk density, showed the best behaviour.
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页码:347 / 352
页数:6
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