SYNTHESIS AND CHARACTERIZATION OF NAC60-CENTER-DOT-5THF

被引:39
作者
DOUTHWAITE, RE [1 ]
BROUGH, AR [1 ]
GREEN, WLH [1 ]
机构
[1] UNIV OXFORD,INORGAN CHEM LAB,OXFORD OX1 3QR,ENGLAND
关键词
D O I
10.1039/c39940000267
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The sodium salt of the monoanion [C-60](-) namely {Na+[C-60](-)(thf)(5)} is prepared and the C-13 and Na-23 solid state NMR, EPR and UV spectra are reported; variable-temperature magnetic susceptibility measurements show a sharp reduction in the magnetic moment below 200 K.
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页码:267 / 268
页数:2
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