VACUUM SUBLIMATION OF POLYNUCLEAR AROMATIC-HYDROCARBONS SEPARATED BY THIN-LAYER CHROMATOGRAPHY FOR DETECTION WITH SHPOLSKII LOW-TEMPERATURE FLUORESCENCE

被引：15

作者：

COLMSJO, A ^{[1
]}

STENBERG, U ^{[1
]}

机构：

[1] UNIV STOCKHOLM, ARRHENIUS LAB, DEPT ANALYT CHEM, S-10691 STOCKHOLM, SWEDEN

来源：

JOURNAL OF CHROMATOGRAPHY | 1979年 / 169卷 / FEB期

关键词：

D O I：

10.1016/0021-9673(75)85045-X

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A method for the vacuum sublimation of polynuclear aromatic hydrocarbons (PAHs) from thin-layer chromatographic plates is described. Low-temperature fluorescence spectroscope, utilizing the Shpol'skii effect, is used for the detection and identification of benzo[a]pyrene, pyrene and benzo[ghi]perylene in samples from different sources. The recoveries of these PAHs were optimized by varying the time and temperature of sublimation. © 1979.

引用

页码：205 / 212

页数：8

共 21 条

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