A METHOD FOR PROTECTION OF HIGHLY REACTIVE METALS DURING EXPOSURE IN AN X-RAY POWDER DIFFRACTION CAMERA

被引:2
作者
BARKER, MG
机构
来源
JOURNAL OF PHYSICS E-SCIENTIFIC INSTRUMENTS | 1969年 / 2卷 / 08期
关键词
D O I
10.1088/0022-3735/2/8/447
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A method is described for the protection of solid alkali metal samples for x-ray diffraction. Examples are given for the preparation and application of a film of polymer to cover the sample. The method has been successfully used for the x-ray diffraction of transition metal wires coated with solid sodium and for powder samples in a matrix of sodium. The technique may be applied to a wide range of compounds and elements which due to their physical and chemical properties may not be handled in the usual manner.
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页码:755 / &
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