FACILE CONVERSION OF PRIMARY AND SECONDARY ALCOHOLS TO ALKYL IODIDES

被引：125

作者：

LANGE, GL

GOTTARDO, C

机构：

[1] Centre for Graduate Work in Chemistry, Depart3193:00:ment of Chemistry and Biochemistry, University of Guelph, Guelph-Waterloo, Ontario

来源：

SYNTHETIC COMMUNICATIONS | 1990年 / 20卷 / 10期

关键词：

D O I：

10.1080/00397919008052864

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A convenient, simple procedure is described for the conversion of a variety of primary and secondary alcohols to iodides in yields ranging from 60-98%, The method employs the Ph3P/imidazole/I2 combination of reagents in the solvent dichloromethane. © 1990, Taylor & Francis Group, LLC. All rights reserved.

引用

页码：1473 / 1479

页数：7

共 16 条

[1] NEW HALOGENATION REAGENT SYSTEMS USEFUL FOR THE MILD ONE-STEP CONVERSION OF ALCOHOLS INTO IODIDES OR BROMIDES
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[3] A PHOSPHORUS NUCLEAR-MAGNETIC-RESONANCE SPECTROSCOPIC STUDY OF THE CONVERSION OF HYDROXY-GROUPS INTO IODO GROUPS IN CARBOHYDRATES USING THE IODINE TRIPHENYLPHOSPHINE IMIDAZOLE REAGENT
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[4] NOVEL REAGENT SYSTEM FOR CONVERTING A HYDROXY-GROUP INTO AN IODO-GROUP IN CARBOHYDRATES WITH INVERSION OF CONFIGURATION .3.
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[5] NOVEL REAGENT SYSTEM FOR CONVERTING A HYDROXY-GROUP INTO AN IODO-GROUP IN CARBOHYDRATES WITH INVERSION OF CONFIGURATION .2.
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[8] REACTION KINETICS + WALDEN INVERSION .PART 10. METHOD FOR ESTIMATING OPTICAL PURITY OF CERTAIN SECONDARY + PRIMARY ALKYL HALIDES . APPLICATION TO 1-METHYLHEPTYL CHLORIDE BROMIDE + IODIDE
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