A CONVENIENT PROCEDURE FOR THE EFFICIENT PREPARATION OF ALKYL (Z)-3-IODO-2-ALKENOATES

被引：65

作者：

PIERS, E

WONG, T

COISH, PD

ROGERS, C

机构：

来源：

CANADIAN JOURNAL OF CHEMISTRY | 1994年 / 72卷 / 08期

关键词：

D O I：

10.1139/v94-230

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Reaction of alkyl 2-alkynoates with sodium iodide (1.6-5.5 equiv.) in acetic acid (6.2-13 equiv.) at 115 degrees C provides good to excellent yields of the corresponding alkyl (Z)-3-iodo-2-alkenoates.

引用

页码：1816 / 1819

页数：4

共 29 条

[1] DIRECT, HIGH-YIELD TRANSFORMATION OF TETRAHYDROPYRANYL ETHERS TO ACETATES
BAKOS, T
VINCZE, I
[J]. SYNTHETIC COMMUNICATIONS, 1989, 19 (3-4) : 523 - 528
[2] BIOUGNE J, 1971, CR ACAD SCI C CHIM, V272, P858
[3] SILICON-DIRECTED NAZAROV CYCLIZATIONS .5. SUBSTITUENT AND HETEROATOM EFFECTS ON THE REACTION
DENMARK, SE
HABERMAS, KL
HITE, GA
[J]. HELVETICA CHIMICA ACTA, 1988, 71 (01) : 168 - 194
[4] BIOMIMETIC SYNTHESIS OF (+/-) PANACENE
FELDMAN, KS
[J]. TETRAHEDRON LETTERS, 1982, 23 (30) : 3031 - 3034
[5] HORMI O, 1988, ORG SYNTH, V66, P173
[6] SIMPLE, STEREOSPECIFIC PREPARATION OF Z-3-IODOACRYLIC ACID FROM PROPIOLIC ACID AND METHYLMAGNESIUM IODIDE
JUNG, ME
HAGENAH, JA
ZENG, LM
[J]. TETRAHEDRON LETTERS, 1983, 24 (37) : 3973 - 3974
[7] A NEW STEREOSELECTIVE SYNTHESIS OF (Z)-VINYLSILANE ALLYLIC ALCOHOLS
KIM, KD
MAGRIOTIS, PA
[J]. TETRAHEDRON LETTERS, 1990, 31 (43) : 6137 - 6140
[8] PREPARATION AND REACTIVITY OF FUNCTIONALIZED ALKENYL-ZINC, ALKENYL-COPPER, AND ALKENYL-CHROMIUM ORGANOMETALLICS
KNOCHEL, P
RAO, CJ
[J]. TETRAHEDRON, 1993, 49 (01) : 29 - 48
[9] PREPARATION AND REACTIONS OF CYCLIC ALLYLIC HIGHER-ORDER CYANOCUPRATES
LIPSHUTZ, BH
UNG, C
ELWORTHY, TR
REUTER, DC
[J]. TETRAHEDRON LETTERS, 1990, 31 (32) : 4539 - 4542
[10] A NOVEL REGIOSPECIFIC AND STEREOSPECIFIC HYDROHALOGENATION REACTION OF 2-PROPYNOIC ACID AND ITS DERIVATIVES
MA, S
LU, XY
LI, ZG
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1992, 57 (02) : 709 - 713

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