SYNTHESIS, PROCESSING AND PROPERTIES OF NANOPHASE ALUMINIDE

被引:22
作者
CHANG, H
HOFLER, J
ALTSTETTER, C
AVERBACK, R
机构
[1] Department of Materials Science and Engineering, University of Illinois at Urbana-Champaign, Champaign, IL
来源
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING | 1992年 / 153卷 / 1-2期
关键词
D O I
10.1016/0921-5093(92)90269-7
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
This paper presents recent results on the production and properties of compacts of ultrafine powders of gamma-TiAl. Metallic vapor was produced by magnetron sputtering of a TiAl target and inert gas-mediated condensation of nanometer sized particles. After collection, the particles were compacted in situ under ultrahigh vacuum conditions. The material was characterized by X-ray diffraction and hardness as a function of sintering time and temperature. Greater than 95% density was achieved in the compacts after sintering for 2 h at 450-degrees-C at which time the average grain size was still less than 20 nm. Hardness was measured as a function of grain size, and normal Hall-Petch behavior was observed, but only at grain sizes above approximately 30 nm, at which point a hardness of 12 GPa was measured. At finer particle sizes the hardness decreased with decreasing grain size.
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页码:676 / 678
页数:3
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