MICRO METHOD FOR THE IDENTIFICATION OF PROANTHOCYANIDIN USING THIOLYSIS MONITORED BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引：167

作者：

RIGAUD, J

PEREZILZARBE, J

RICARDO-DA-SILVA, JM

CHEYNIER, V

机构：

[1] Institut National de la Recherche Agronomique, Institut des Produits de la Vigne, Laboratoire des Polymères et des Techniques Physico-chimiques, 34060 Montpellier Cedex

来源：

JOURNAL OF CHROMATOGRAPHY | 1991年 / 540卷 / 1-2期

关键词：

D O I：

10.1016/S0021-9673(01)88830-0

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The classical method of procyanidin thiolysis was modified so as to render it suitable for the identification of small amounts (< 0.1 mg) of compound. High-performance liquid chromatographic monitoring of the degradation kinetics gives access to the intermediate products. The use of sulphur dioxide instead of acetic acid as the hydrolysing agent allows a faster reaction, thus minimizing structural modifications, and prevents alterations due to procyanidin oxidation.

引用

页码：401 / 405

页数：5

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