COMPLETE H-1 AND C-13 NMR SPECTRAL ASSIGNMENT OF SOME POLYNITROPOLYCYCLIC CAGE MOLECULES BY 2D NMR-SPECTROSCOPY

被引：6

作者：

AXENROD, T ^{[1
]}

LIANG, B ^{[1
]}

DAVE, PR ^{[1
]}

机构：

[1] ARDEC,GEO CTR INC,LAKE HOPATCONG,NJ 07849

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 1991年 / 29卷 / 01期

关键词：

POLYNITROPOLYCYCLIC MOLECULES; AROMATIC SOLVENT-INDUCED SHIFTS; NOE DIFFERENCE SPECTRA; 2D LONG-RANGE C-13-H-1 SHIFT CORRELATED SPECTRA; NITROSUBSTITUTED ADAMANTANES; NITROSUBSTITUTED PENTACYCLOUNDECANES;

D O I：

10.1002/mrc.1260290104

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The H-1 and C-13 NMR spectra of several saturated polynitropolycyclic molecules were unambiguously assigned using aromatic solvent-induced shifts, NOE difference spectra, H-1-H-1 COSY spectra and 2D C-13-H-1 shift correlated spectra, optimized either for one-bond or long-range C-13-H-1 couplings.

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页码：9 / 17

页数：9

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