EFFECT OF MATRIX ON THE DETERMINATION OF VOLATILE METALS IN BIOLOGICAL SAMPLES BY FLAMELESS ATOMIC-ABSORPTION SPECTROMETRY WITH THE GRAPHITE TUBE ATOMIZER

被引：11

作者：

ISSAQ, HJ

机构：

[1] Chemical Carcinogenesis Program, NCI Frederick Cancer Research Center, Frederick

来源：

ANALYTICAL CHEMISTRY | 1979年 / 51卷 / 06期

关键词：

D O I：

10.1021/ac50042a017

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The effect of varying the matrix, ashing temperature, or digesting agent on the determination of the amount of volatile metals in biological samples was studied. The results showed that changing these parameters can affect the accuracy of the measurements. While it was found that an ashing temperature above 600 °C is impractical for the determination of Pb, Cd and Zn in biological samples, no loss of signal occurred when these compounds were analyzed in an aqueous solution. © 1979, American Chemical Society. All rights reserved.

引用

页码：657 / 659

页数：3

共 7 条

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FERNANDEZ FJ, 1975, CLIN CHEM, V21, P558

[2] LOSS OF LEAD FROM AQUEOUS-SOLUTIONS DURING STORAGE [J].

ISSAQ, HJ ;

ZIELINSK.WL .

ANALYTICAL CHEMISTRY, 1974, 46 (09) :1328-1329

[3] MODIFICATION OF A GRAPHITE TUBE ATOMIZER FOR FLAMELESS ATOMIC-ABSORPTION SPECTROMETRY [J].

ISSAQ, HJ ;

ZIELINSKI, WL .

ANALYTICAL CHEMISTRY, 1975, 47 (13) :2281-2283

[4]

ISSAQ HJ, UNPUBLISHED

[5]

KUBASIK NP, 1972, CLIN CHEM, V18, P410

[6]

MORGENTHALER LP, 1978, COMMUNICATION

[7]

MORGENTHALER LP, 1978, 29TH PITTSB C ANAL C

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