DETERMINATION OF 54MN IN FOODS

被引:4
作者
DAVIS, S
ARNOLD, A
JORDAN, A
机构
[1] Division of Pharmacology, Food and Drug Administration, Washington, D. C.
来源
JOURNAL OF RADIOANALYTICAL CHEMISTRY | 1969年 / 2卷 / 3-4期
关键词
D O I
10.1007/BF02513726
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
54Mn is analyzed in complex food ash of high cationic environment. The initial step is an extraction at pH 2.7 with hexane containing di(2-ethylhexyl) phosphoric acid (HDEHP) to complex the54Mn and other nuclides. The manganese is reextracted into an alkaline EDTA buffer which is washed with 1% 8-hydroxyquinoline in chloroform containing 5% isoamyl alcohol. The54Mn is determined by gamma spectrometry with recoveries ranging from 96.6 to 99.4%. © 1969 Akadémiai Kiadó.
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页码:161 / &
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