A GENERAL-APPROACH TO UNSYMMETRICAL TRICOORDINATE IODINANES - SINGLE STEP PREPARATION OF MIXED IODOSOBENZENE SULFONATES PHI(X)OSO2R, VIA REACTION OF IODOSOBENZENE WITH ME3SIX

被引：61

作者：

ZHDANKIN, VV

CRITTELL, CM

STANG, PJ

ZEFIROV, NS

机构：

[1] UNIV UTAH,DEPT CHEM,SALT LAKE CITY,UT 84112

[2] MOSCOW MV LOMONOSOV STATE UNIV,DEPT CHEM,MOSCOW 119899,RUSSIA

来源：

TETRAHEDRON LETTERS | 1990年 / 31卷 / 34期

基金：

美国国家卫生研究院;

关键词：

D O I：

10.1016/S0040-4039(00)97741-4

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Mixed iodonium sulfonates of the type Phl(X)OSO2R (X = OAc, NHAc, NCO, CN; R = CF3, C4F9, p-CH3C6H4) have been prepared by the reaction of PhlO with the appropriate derivatives of trimethylsilane. © 1990.

引用

页码：4821 / 4824

页数：4

共 18 条

[1]

HEMBRE RT, 1987, J ORG CHEM, V52, P1650

[2] ONE-STEP ALPHA-TOSYLOXYLATION OF KETONES WITH [HYDROXY(TOSYLOXY)IODO]BENZENE [J].

KOSER, GF ;

RELENYI, AG ;

KALOS, AN ;

REBROVIC, L ;

WETTACH, RH .

JOURNAL OF ORGANIC CHEMISTRY, 1982, 47 (12) :2487-2489

[3] HYPERVALENT ORGANOIODINE - REACTIONS OF SILVER ARYLSULFONATES WITH IODOSOBENZENE DICHLORIDE [J].

KOSER, GF ;

WETTACH, RH .

JOURNAL OF ORGANIC CHEMISTRY, 1977, 42 (08) :1476-1478

[4] DIRECT ALPHA-MESYLOXYLATION OF KETONES AND BETA-DICARBONYL COMPOUNDS WITH [HYDROXY(MESYLOXY)IODO]BENZENE [J].

LODAYA, JS ;

KOSER, GF .

JOURNAL OF ORGANIC CHEMISTRY, 1988, 53 (01) :210-212

[5]

MERKUSHEV EB, 1987, RUSS CHEM REV, V56, P826

[6] HYPERVALENT IODINE IN ORGANIC-SYNTHESIS [J].

MORIARTY, RM ;

PRAKASH, O .

ACCOUNTS OF CHEMICAL RESEARCH, 1986, 19 (08) :244-250

[7] REACTION OF [HYDROXY(TOSYLOXY)IODO]BENZENE AND [HYDROXY(MESYLOXY)IODO]BENZENE WITH TRIMETHYLSILYL ENOL ETHERS - A NEW GENERAL-METHOD FOR ALPHA-SULFONYLOXYLATION OF CARBONYL-COMPOUNDS [J].

MORIARTY, RM ;

PENMASTA, R ;

AWASTHI, AK ;

EPA, WR ;

PRAKASH, I .

JOURNAL OF ORGANIC CHEMISTRY, 1989, 54 (05) :1101-1104

[8]

MORIARTY RM, IN PRESS SYNLETT

[9]

NEILAND O, 1970, ZH ORG KHIM+, V6, P889

[10] HYPERVALENT ORGANOIODINE COMPOUNDS IN ORGANIC-SYNTHESIS - REACTION WITH ORGANOSILICON AND TIN [J].

OCHIAI, M ;

NAGAO, Y .

JOURNAL OF SYNTHETIC ORGANIC CHEMISTRY JAPAN, 1986, 44 (07) :660-673

← 1 2 →